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Beilstein J. Org. Chem. 2012, 8, 1118–1125, doi:10.3762/bjoc.8.124
Graphical Abstract
Figure 1: Smectic A phase of a mixture of two mesogens differing strongly in molecular length. Left: The laye...
Scheme 1: Chemical structures and phase-transition temperatures of the mesogens 2PhP and PhP16 and of the chi...
Figure 2: Molecular structures and molecular lengths of 2PhP and PhP16. The longer mesogen PhP16 is approxima...
Figure 3: The phase diagram of the binary mixture system PhP16/2PhP.
Figure 4: The layer spacing obtained by SAXS-measurements in the SmA phase at T = Tc is plotted against the m...
Figure 5: Reduced layer spacing d/dA versus temperature difference to the phase-transition temperature T−Tc f...
Figure 6: The tilt angle θ is plotted against the temperature difference to the phase-transition temperature T...
Figure 7: Translational order parameter Σ in the SmA phase versus temperature difference to the phase-transit...
Figure 8: Textures of the pure compound PhP16 on cooling. Left: SmC phase at 96.8 °C Right: same positions in...
Figure 9: Integrated intensity profile of an unoriented sample of PhP16 at T = 82.5 °C in the SmF phase.
Figure 10: (a) WAXS-measurement of the SmF phase of PhP16 at T = 82 °C with the smectic-layer normal k oriente...
Figure 11: (a) WAXS-measurement of the SmF phase of PhP16 at T = 88 °C with the smectic layer normal oriented ...
Figure 12: (a) Layer spacing of the SmF and the SmC phase of the pure compound PhP16 in dependence of the temp...